Rapid one-pot synthesis of cycloheptatriene-phosphonium.
The X-ray crystal structure of dibenzo-24-crown-8 (2B24C8) with tropylium tetrafluoroborate inclusion complex was determined, giving the following crystal data: 2B24C8-TrBF4 (C31H39O8. 0.5 CH3CN.
Tropylium tetrafluoroborate reacts with tertiary carbanions bearing leaving groups at the carbanionic center yielding covalent adducts. Some of them can be transformed into heptafulvenes or tropyli.
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